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| techniques in organic chemistry: Techniques in Organic Chemistry Jerry R. Mohrig, Christina Noring Hammond, Paul F. Schatz, 2010-01-06 Compatible with standard taper miniscale, 14/10 standard taper microscale, Williamson microscale. Supports guided inquiry--Cover. |
| techniques in organic chemistry: Laboratory Techniques in Organic Chemistry Jerry R. Mohrig, David Alberg, Gretchen Hofmeister, Paul F. Schatz, Christina Noring Hammond, 2014-03-01 Laboratory Techniques in Organic Chemistry is the most comprehensive and detailed presentation of the lab techniques organic chemistry students need to know. Compatible with any organic chemistry lab manual or set of experiments, it combines specific instructions for three different kinds of laboratory glassware: miniscale, standard taper microscale, and Williamson microscale. It is written to provide effective support for guided-inquiry and design-based experiments and projects, as well as for traditional lab experiments. |
| techniques in organic chemistry: High-resolution NMR Techniques in Organic Chemistry T. Claridge, 1999-12-24 From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book. |
| techniques in organic chemistry: Techniques and Experiments for Organic Chemistry Addison Ault, 1994 |
| techniques in organic chemistry: The Organic Chem Lab Survival Manual James W. Zubrick, 2020-02-05 Teaches students the basic techniques and equipment of the organic chemistry lab — the updated new edition of the popular hands-on guide. The Organic Chem Lab Survival Manual helps students understand the basic techniques, essential safety protocols, and the standard instrumentation necessary for success in the laboratory. Author James W. Zubrick has been assisting students navigate organic chemistry labs for more than three decades, explaining how to set up the laboratory, make accurate measurements, and perform safe and meaningful experiments. This practical guide covers every essential area of lab knowledge, from keeping detailed notes and interpreting handbooks to using equipment for chromatography and infrared spectroscopy. Now in its eleventh edition, this guide has been thoroughly updated to cover current laboratory practices, instruments, and techniques. Focusing primarily on macroscale equipment and experiments, chapters cover microscale jointware, drying agents, recrystallization, distillation, nuclear magnetic resonance, and much more. This popular textbook: Familiarizes students with common lab instruments Provides guidance on basic lab skills and procedures Includes easy-to-follow diagrams and illustrations of lab experiments Features practical exercises and activities at the end of each chapter Provides real-world examples of lab notes and instrument manuals The Organic Chem Lab Survival Manual: A Student’s Guide to Techniques, 11th Edition is an essential resource for students new to the laboratory environment, as well as those more experienced seeking to refresh their knowledge. |
| techniques in organic chemistry: Practical Synthetic Organic Chemistry Stéphane Caron, 2020-02-05 Diese Publikation ist ein Praktikerbuch für Organiker. Der Schwerpunkt liegt auf den Reaktionen, die am verlässlichsten und nützlichsten sind. Die Autoren der einzelnen Kapitel stellen Chemiker die Informationen zur Verfügung, die für die strategische Planung einer Synthese und Wiederholung der Verfahren im Labor notwendig sind. - Fasst alle wesentlichen Entwicklungen und Konzepte in einer Publikation zusammen und deckt die meisten der wichtigen Reaktionen in der organischen Chemie ab, u. a. Substitutions-, Additions-, Eliminierungsreaktionen, Umlagerung, Oxidation, Reduktion. - Behandelt die wichtigsten Reaktionen ausführlicher und zeigt die grundlegenden Prinzipien, Vor- und Nachteile der Methoden, Mechanismen und Techniken, um Reaktionen im Labor erfolgreich durchzuführen. - Mit neuen Inhalten zu den jüngsten Fortschritten in den Bereichen CH-Aktivierung, Photoredox-Katalyse und Elektrochemie, kontinuierliche chemische Prozesse und Anwendung der Biokatalyse in der Synthese. - Bietet überarbeitete Kapitel mit neuen und zusätzlichen chemischen Beispielen aus der Praxis. |
| techniques in organic chemistry: The Student's Lab Companion John W. Lehman, 2008 This comprehensive lab companion provides enough theory to help students understand how and why an operation works, but emphasizes the practical aspects of an operation to help them perform the operation successfully in the lab. For undergraduate or graduate students taking organic chemistry lab. This comprehensive lab companion provides enough theory to help students understand how and why an operation works, but emphasizes the practical aspects of an operation to help them perform the operation successfully in the lab. The Second Edition makes substantive revisions of many operations to clarify existing material and add new information. More environmentally friendly (i.e. ? green? ) lab experiments are encouraged. Ideal for professors who write their own lab experiments or would like custom labs but need a source for lab operations and safety information. |
| techniques in organic chemistry: Organic Laboratory Techniques Ralph J. Fessenden, Joan S. Fessenden, Patty Feist, 2001 This highly effective and practical manual is designed to be used as a supplementary text for the organic chemistry laboratory course - and with virtually any main text - in which experiments are supplied by the instructor or in which the students work independently. Each technique contains a brief theoretical discussion. Steps used in each technique, along with common problems that might arise. These respected and renowned authors include supplemental or related procedures, suggested experiments, and suggested readings for many of the techniques. Additionally, each chapter ends with a set of study problems that primarily stress the practical aspects of each technique, and microscale techniques are included throughout the text, as appropriate. Additional exercises, reference material, and quizzes are available online. |
| techniques in organic chemistry: Basic Techniques of Preparative Organic Chemistry William Sabel, 2013-09-03 Basic Techniques of Preparative Organic Chemistry covers a detailed guide for carrying out the procedures commonly needed in preparative organic chemistry. The book discusses the nature of organic reactions; the basic principles of preparative organic chemistry; unit operations; and good laboratory practice. The text then provides a review of apparatus and equipment and describes the potential hazards involved in a chemical operation, such as toxicity, bodily injuries, smoking, fire, explosion, and implosion. Techniques and unit operations for carrying out a reaction and for isolating and purifying a reaction product; and the criteria for and methods of assessing purity are also considered. The book further tackles packing and storing products and samples and making reports and communications. Students taking organic chemistry courses will find the text useful. |
| techniques in organic chemistry: Practical Synthetic Organic Chemistry Stéphane Caron, 2011-08-16 A hands-on guide to assist in the planning and execution of synthetic reactions in the laboratory Despite the maturity of organic chemistry, it can still be very challenging to identify optimal methods for synthetic transformations that perform as well in real-world manufacturing processes as they do in the laboratory. This detailed and accessible guide attempts to address this vexing issue and deliver proven methodologies practicing synthetic chemists will find valuable for identifying reaction conditions that work reliably over the broadest possible range of substrates. Practical Synthetic Organic Chemistry: Provides a practical guide to strategically planning and executing chemical syntheses for the bench chemist in industry Discusses information that is not common knowledge beyond the boundaries of process chemistry groups, such as the synthetic routes of selected contemporary pharmaceutical drugs and practical solvents, as well as green chemistry concepts Highlights key reactions, including substitutions, additions, eliminations, rearrangements, oxidations, and reductions Addresses basic principles, mechanisms, advantages and disadvantages of the methodology, and techniques for achieving laboratory success Incorporating such an extraordinary wealth of information on organic chemistry and its related fields into one complete volume distinguishes Practical Synthetic Organic Chemistry as an incomparable desktop reference for professionals—and an invaluable study aid for students. |
| techniques in organic chemistry: Spectroscopic Methods in Organic Chemistry Dudley H. Williams, Ian Fleming, 1980 |
| techniques in organic chemistry: Techniques and Experiments for Organic Chemistry Ralph J. Fessenden, Joan S. Fessenden, 1983 |
| techniques in organic chemistry: Making the Connections3 Anne B. Padias, 2015 |
| techniques in organic chemistry: Purification of Laboratory Chemicals W.L.F. Armarego, 2003-03-07 Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.* Complete update of this valuable, well-known reference* Provides purification procedures of commercially available chemicals and biochemicals* Includes an extremely useful compilation of ionisation constants |
| techniques in organic chemistry: Organic Laboratory Techniques Ralph J. Fessenden, Joan S. Fessenden, 1984 |
| techniques in organic chemistry: Techniques and Experiments for Advanced Organic Laboratory Charles M. Garner, 1997-01-02 This book introduces chemists to a variety of techniques which are used in the organic laboratory, including key instrumental analyses such as NMR, capillary GC and GC-MS. Several of the methods, particularly capillary GC and NMR, illustrate the power of modern instrumentation. |
| techniques in organic chemistry: Experiments and Techniques in Organic Chemistry Daniel J. Pasto, 1992 |
| techniques in organic chemistry: Practical Organic Chemistry J.T. Sharp, 2012-12-06 One of the very best things about organic chemistry is actually doing experimental work at the beneh. This applies not only at the profes sionallevel but also from the earliest stages of apprenticeship to the craft as a student. The fascination sterns from the nature of the sub ject itself, with its vast array of different types of reaction and its al most infinite variety of different chemical compounds. Each reaction and each new compound pose their own particular problems to chal lenge the skill and ingenuity of the chemist, whether working in a first-year teaching la bora tory or at the frontiers of research. This book is intended to provide basic guidance in the essential experimental techniques used in a typical undergraduate course. It gives concise coverage of the range of practical skills required, from first-year level when students may have no previous experience, up to final-year level when students are usually involved in more complex and dem an ding experimental workin supervised research projects. Our objective was to produce a handbook of techniques that could be used with a variety of practical courses throughout a student's whole period of study. Those who run practical courses generally have strong feelings about what particular experiments or exercises are appropriate for their own students, and it is rare that a book of experiments suitable for one department is acceptable to another. |
| techniques in organic chemistry: Organic Chemistry of Museum Objects John Mills, Raymond White, 2012-09-10 'The Organic Chemistry of Museum Objects' makes available in a single volume, a survey of the chemical composition, properties and analysis of the whole range of organic materials incorporated into objects and artworks found in museum collections. The authors cover the fundamental chemistry of the bulk materials such as wood, paper, natural fibres and skin products, as well as that of the relatively minor components incorporated as paint, media, varnishes, adhesives and dyes. This expanded second edition, now in paperback, follows the structure of the first, though it has been extensively updated. In addition to chapters on basic organic chemistry, analytical methods, analytical findings and fundamental aspects of deterioration, the subject matter is grouped as far as possible by broad chemical class - oils and fats, waxes, bitumens, carbohydrates, proteins, natural resins, dyestuffs and synthetic polymers. This is an essential purchase for all practising and student conservators, restorers, museum scientists, curators and organic chemists. |
| techniques in organic chemistry: Advanced Organic Synthesis Richard Monson, 2012-12-02 Advanced Organic Synthesis: Methods and Techniques presents a survey and systematic introduction to the modern techniques of organic synthesis. The book attempts to acquaint the reader with a variety of laboratory techniques as well as introduce chemical reagents that require deftness and care in handling. Chapters are devoted that discuss the techniques of organic synthesis; apparatus and terminology used in the description of synthetic procedures; the scope and mechanism of chemical reactions; and technical procedures on how to perform chemical experiments. The text will be of vital importance to advanced undergraduate student or beginning graduate student of chemistry. |
| techniques in organic chemistry: Experiments in Organic Chemistry F.R. Lorriman, J.J. Rae, G.H. Schmid, 1966-12-15 The experiments in this book are designed for students beginning the study of organic chemistry. The purposes of the book are to teach the student some of the techniques of organic chemistry and to familiarize him with the methods of preparation and chemical properties of representative members of the important classes of organic compounds. Each section contains a brief introduction to that part of the work and should help the student to understand the subsequent experiments. |
| techniques in organic chemistry: Organic Chemistry with Vernier Elaine Y. Nam, Melissa P. Hill, Jack Randall, 2018-12-30 |
| techniques in organic chemistry: A Microscale Approach to Organic Laboratory Techniques Donald L. Pavia, George S. Kriz, Gary M. Lampman, Randall G. Engel, 2016-12-05 Featuring new experiments unique to this lab textbook, as well as new and revised essays and updated techniques, this Sixth Edition provides the up-to-date coverage students need to succeed in their coursework and future careers. From biofuels, green chemistry, and nanotechnology, the book’s experiments, designed to utilize microscale glassware and equipment, demonstrate the relationship between organic chemistry and everyday life, with project-and biological or health science focused experiments. As they move through the book, students will experience traditional organic reactions and syntheses, the isolation of natural products, and molecular modeling. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version. |
| techniques in organic chemistry: Modern NMR Techniques for Chemistry Research A.E. Derome, 2013-10-22 Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR. |
| techniques in organic chemistry: Introduction to Organic Laboratory Techniques Donald L. Pavia, Gary M. Lampman, George S. Kriz, Randall G. Engel, 2005 Featuring 66 experiments, detailing 29 techniques, and including several explicating essays, this lab manual covers basic lab techniques, molecular modeling, properties and reactions of organic compounds, the identification of organic substances, project-based experiments, and each step of the various techniques. The authors teach at Western Washington University and North Seattle Community College. Annotation ♭2004 Book News, Inc., Portland, OR (booknews.com). |
| techniques in organic chemistry: Comprehensive Organic Chemistry Experiments for the Laboratory Classroom Carlos A. M. Afonso, Nuno R. Candeias, Dulce Pereira Simão, Alexandre F. Trindade, Jaime A. S. Coelho, Bin Tan, Robert Franzén, 2016-12-16 This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students. |
| techniques in organic chemistry: Experimental Organic Chemistry Philippa B. Cranwell, Laurence M. Harwood, Christopher J. Moody, 2017-08-14 The definitive guide to the principles and practice of experimental organic chemistry - fully updated and now featuring more than 100 experiments The latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. All sections have been updated to reflect new techniques, equipment and technologies, and the text has been revised with an even sharper focus on practical skills and procedures. The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis. The second half contains step-by-step experimental procedures, each one illustrating a basic principle, or important reaction type. Tried and tested over almost three decades, over 100 validated experiments are graded according to their complexity and all are chosen to highlight important chemical transformations and to teach key experimental skills. New sections cover updated health and safety guidelines, additional spectroscopic techniques, electronic notebooks and record keeping, and techniques, such as semi-automated chromatography and enabling technologies such as the use of microwave and flow chemistry. New experiments include transition metal-catalysed cross-coupling, organocatalysis, asymmetric synthesis, flow chemistry, and microwave-assisted synthesis. Key aspects of this third edition include: Detailed descriptions of the correct use of common apparatus used in the organic laboratory Outlines of practical skills that all chemistry students must learn Highlights of aspects of health and safety in the laboratory, both in the first section and throughout the experimental procedures Four new sections reflecting advances in techniques and technologies, from electronic databases and information retrieval to semi-automated chromatography More than 100 validated experiments of graded complexity from introductory to research level A user-friendly experiment directory An instructor manual and PowerPoint slides of the figures in the book available on a companion website A comprehensive guide to contemporary organic chemistry laboratory principles, procedures, protocols, tools and techniques, Experimental Organic Chemistry, Third Edition is both an essential laboratory textbook for students of chemistry at all levels, and a handy bench reference for experienced chemists. |
| techniques in organic chemistry: Laboratory Techniques in Organic Chemistry V. K. Ahluwalia, 2013-12-30 This book deals with general information about work in Organic Chemistry Laboratory, viz., safety, first aid, different types of apparatus and their assemblies used for various types of reactions, stirring arrangements, heating techniques and low temperature experiments. Various methods used for purification of organic compounds have been described. Besides the normal technique, the book includes write-up about molecular distillation, chromatography and electrophoresis. Special emphasis has been given to the methods, which can be used for working up of organic reactions. Various methods, which can be used successfully for isolation of products from natural sources, have been incorporated. Emphasis has also been given on the isolation of products from oily mixture using the technique of Liquid-Liquid extraction. Methods for determining the criteria of purity of organic compounds have been discussed. The book also deals with drying and purification of solvents, preparation of spectroscopical grade solvents and HPCL solvents. The preparation of commonly used deuterated solvents (which are used for NMR spectroscopy work) is a special feature of this book. |
| techniques in organic chemistry: New Methodologies and Techniques for a Sustainable Organic Chemistry Alessandro Mordini, Ferenc Faigl, 2008-04-17 Chemical industries have to face the big challenge of finding adequate processes to produce large quantities of new products for which there is a present need, decreasing at the same time both the impact on the environment and the risk of disasters. These issues have led to the establishment of new concepts of sustainable development as affirmed in the Rio Declaration on Environment and Development in the early 90’s and has been the subject of intensive studies in the last two decades. The book addresses this challenge collecting the recent “New Methodologies and Techniques for a Sustainable Organic Chemistry”. It provides a wealth of information in the fields of - New efficient and selective catalytic processes - Use of non-usual media or environmentally benign reagents - New selective and efficient synthetic methods - New techniques based on alternative energy sources. All these topics are covered in 15 chapters written by world-renowned experts in these fields who were the lecturers of the NATO ASI NeMeTOC (2005, Siena). Since some of the authors have an industrial background, the book helps to answer virtually any questions which may arise during the development of a new environmentally benign organic process. |
| techniques in organic chemistry: Green Organic Chemistry in Lecture and Laboratory Andrew P. Dicks, 2016-04-19 The last decade has seen a huge interest in green organic chemistry, particularly as chemical educators look to green their undergraduate curricula. Detailing published laboratory experiments and proven case studies, this book discusses concrete examples of green organic chemistry teaching approaches from both lecture/seminar and practical perspe |
| techniques in organic chemistry: The Organic Chemistry of Drug Design and Drug Action Richard B. Silverman, 2012-12-02 Standard medicinal chemistry courses and texts are organized by classes of drugs with an emphasis on descriptions of their biological and pharmacological effects. This book represents a new approach based on physical organic chemical principles and reaction mechanisms that allow the reader to extrapolate to many related classes of drug molecules. The Second Edition reflects the significant changes in the drug industry over the past decade, and includes chapter problems and other elements that make the book more useful for course instruction. - New edition includes new chapter problems and exercises to help students learn, plus extensive references and illustrations - Clearly presents an organic chemist's perspective of how drugs are designed and function, incorporating the extensive changes in the drug industry over the past ten years - Well-respected author has published over 200 articles, earned 21 patents, and invented a drug that is under consideration for commercialization |
| techniques in organic chemistry: Essential Practical NMR for Organic Chemistry S. A. Richards, J. C. Hollerton, 2010-12-07 This book describes the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation. It features a significant amount of vital chemical shift and coupling information but more importantly, it presents sound principles for the selection of the techniques relevant to the solving of particular types of problem, whilst stressing the importance of extracting the maximum available information from the simple 1-D proton experiment and of using this to plan subsequent experiments. Proton NMR is covered in detail, with a description of the fundamentals of the technique, the instrumentation and the data that it provides before going on to discuss optimal solvent selection and sample preparation. This is followed by a detailed study of each of the important classes of protons, breaking the spectrum up into regions (exchangeables, aromatics, heterocyclics, alkenes etc.). This is followed by consideration of the phenomena that we know can leave chemists struggling; chiral centres, restricted rotation, anisotropy, accidental equivalence, non-first-order spectra etc. Having explained the potential pitfalls that await the unwary, the book then goes on to devote chapters to the chemical techniques and the most useful instrumental ones that can be employed to combat them. A discussion is then presented on carbon-13 NMR, detailing its pros and cons and showing how it can be used in conjunction with proton NMR via the pivotal 2-D techniques (HSQC and HMBC) to yield vital structural information. Some of the more specialist techniques available are then discussed, i.e. flow NMR, solvent suppression, Magic Angle Spinning, etc. Other important nuclei are then discussed and useful data supplied. This is followed by a discussion of the neglected use of NMR as a tool for quantification and new techniques for this explained. The book then considers the safety aspects of NMR spectroscopy, reviewing NMR software for spectral prediction and data handling and concludes with a set of worked Q&As. |
| techniques in organic chemistry: March's Advanced Organic Chemistry Michael B. Smith, Jerry March, 2007-01-29 The Sixth Edition of a classic in organic chemistry continues its tradition of excellence Now in its sixth edition, March's Advanced Organic Chemistry remains the gold standard in organic chemistry. Throughout its six editions, students and chemists from around the world have relied on it as an essential resource for planning and executing synthetic reactions. The Sixth Edition brings the text completely current with the most recent organic reactions. In addition, the references have been updated to enable readers to find the latest primary and review literature with ease. New features include: More than 25,000 references to the literature to facilitate further research Revised mechanisms, where required, that explain concepts in clear modern terms Revisions and updates to each chapter to bring them all fully up to date with the latest reactions and discoveries A revised Appendix B to facilitate correlating chapter sections with synthetic transformations |
| techniques in organic chemistry: Nomenclature of Organic Chemistry Henri A Favre, Warren H Powell, 2013-12-05 Chemical nomenclature is used to identify a chemical species by means of written or spoken words and enables a common language for communication amongst chemists. Nomenclature for chemical compounds additionally contains an explicit or implied relationship to the structure of the compound, in order that the reader or listener can deduce the structure from the name. This purpose requires a system of principles and rules, the application of which gives rise to a systematic nomenclature. Of course, a wide range of traditional names, semisystematic or trivial, are also in use for a core group of common compounds. Detailing the latest rules and international practice, this new volume can be considered a guide to the essential organic chemical nomenclature, commonly described as the Blue Book. An invaluable source of information for organic chemists everywhere and the definitive guide for scientists working in academia or industry, for scientific publishers of books, journals and databases, and for organisations requiring internationally approved nomenclature in a legal or regulatory environment. |
| techniques in organic chemistry: Organic and Inorganic Fluorine Chemistry Axel Haupt, 2021-03-22 Organic and Inorganic Fluorine Chemistry provides an introduction to fluorine chemistry and an overview of the most important fluorinated compounds and general preparation techniques. The book is divided into three parts, covering general aspects, inorganic fluorides and fluoroorganic compounds. The inorganic part presents the most important element fluorides and oxyfluorides, their preparation as well as their most characteristic properties. The organic section focuses on the different types of fluorination and the corresponding reagents. The application of these techniques is discussed for many different types of substrates. The book addresses advanced students in chemistry as well as researchers in academia and industry. The readers will benefit from a large number of original references which give access to further information. In addition, study questions at the end of each chapter will help to repeat and internalise the most important aspects. |
| techniques in organic chemistry: Fundamentals of Analytical Chemistry Douglas A. Skoog, Donald M. West, 1982 |
| techniques in organic chemistry: Modern NMR Techniques for Synthetic Chemistry Julie Fisher, 2014-10-13 A blend of theory and practical advice, Modern NMR Techniques for Synthetic Chemistry illustrates how NMR spectroscopy can be used to determine the abundance, size, shape, and function of organic molecules. It provides you with a description the NMR technique used (more pictorial than mathematical), indicating the most common pulse sequences, some practical information as appropriate, followed by illustrative examples. This format is followed for each chapter so you can skip the more theoretical details if the practical aspects are what interest you. Following a discussion of basic parameters, the book describes the utility of NMR in detecting and quantifying dynamic processes, with particular emphasis on the usefulness of saturation-transfer (STD) techniques. It details pulsed–field gradient approaches to diffusion measurement, diffusion models, and approaches to ‘inorganic’ nuclei detection, important as many synthetic pathways to new organics involve heavier elements. The text concludes with coverage of applications of NMR to the analysis of complex mixtures, natural products, carbohydrates, and nucleic acids—all areas of activity for researchers working at the chemistry-life sciences interface. The book’s unique format provides some theoretical insight into the NMR technique used, indicating the most common pulse sequences. The book draws upon several NMR methods that are resurging or currently hot in the field and indicates the specific pulse sequence used by various spectrometer manufacturers for each technique. It examines the analysis of complex mixtures, a feature not found in most books on this topic. |
| techniques in organic chemistry: Advanced Organic Chemistry Francis A. Carey, Richard J. Sundberg, 2007-06-27 Since its original appearance in 1977, Advanced Organic Chemistry has maintained its place as the premier textbook in the field, offering broad coverage of the structure, reactivity and synthesis of organic compounds. As in the earlier editions, the text contains extensive references to both the primary and review literature and provides examples of data and reactions that illustrate and document the generalizations. While the text assumes completion of an introductory course in organic chemistry, it reviews the fundamental concepts for each topic that is discussed. The two-part fifth edition has been substantially revised and reorganized for greater clarity. Among the changes: Updated material reflecting advances in the field since 2001’s Fourth Edition, especially in computational chemistry; A companion Web site provides digital models for study of structure, reaction and selectivity; Solutions to the exercises provided to instructors online. The material in Part Ais organized on the basis of fundamental structural topics such as structure, stereochemistry, conformation and aromaticity and basic mechanistic types, including nucleophilic substitution, addition reactions, carbonyl chemistry, aromatic substitution and free radical reactions. Together with Part B: Reaction and Synthesis, the two volumes are intended to provide the advanced undergraduate or beginning graduate student in chemistry with a sufficient foundation to comprehend and use the research literature in organic chemistry. |
| techniques in organic chemistry: Laboratory Technique in Organic Chemistry Kenneth B. Wiberg, 1960 |
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TECHNIQUE Definition & Meaning - Merriam-Webster
The meaning of TECHNIQUE is the manner in which technical details are treated (as by a writer) or basic physical movements are used (as by a dancer); also : ability to treat such details or …
TECHNIQUE | English meaning - Cambridge Dictionary
Yoga is a very effective technique for combating stress. I refuse to be intimidated by high-pressure sales techniques. We ensure that our surgeons are trained in all the latest surgical techniques. …
TECHNIQUE Definition & Meaning - Dictionary.com
method of performance; way of accomplishing. technical skill; ability to apply procedures or methods so as to effect a desired result. Informal. method of projecting personal charm, …
technique - Oxford Learner's Dictionaries
Definition of technique noun from the Oxford Advanced Learner's Dictionary. [countable] a particular way of doing something, especially one in which you have to learn special skills. …
TECHNIQUE definition and meaning | Collins English Dictionary
A technique is a particular method of doing an activity, usually a method that involves practical skills. ...tests performed using a new technique. Technique is skill and ability in an artistic, …
Technique - definition of technique by The Free Dictionary
1. the manner and ability with which an artist, writer, athlete, etc., employs the technical skills of a particular art or field of endeavor. 2. the body of specialized procedures and methods used in …
Technique Definition & Meaning - YourDictionary
Technique definition: The basic method for making or doing something, such as an artistic work or scientific procedure.
